Isoprocarb synthesis
- Product Name:Isoprocarb
- CAS Number:2631-40-5
- Molecular formula:C11H15NO2
- Molecular Weight:193.24
88-69-7
195 suppliers
$5.00/5 g
105-40-8
93 suppliers
$40.00/250mg
2631-40-5
168 suppliers
$98.29/50mg
Yield:-
Reaction Conditions:
with trichlorophosphate in toluene
Steps:
9 2-ISOPROPYLPHENYL N-METHYLCARBAMATE
EXAMPLE 9 2-ISOPROPYLPHENYL N-METHYLCARBAMATE To a solution of 2-isopropylphenol (1.38 g, 0.01 mole) and ethyl N-methylcarbamate (1.03 g, 0.01 mole) in toluene (10 ml), was added phosphoryl chloride (1.54 g, 0.01 mole) and refluxed for six hours. The reaction mixture was worked up as described earlier to give 2-isopropylphenyl N-methylcarbamate as a solid, crystallized from petroleum ether, m.p. 88oC to 93oC.
References:
Council of Scientific and, Industrial Research EP446514, 1991, A1
88-69-7
195 suppliers
$5.00/5 g
2631-40-5
168 suppliers
$98.29/50mg