ISOPROPYLPHENYL SULFONE synthesis

9synthesis methods

Product Name:ISOPROPYLPHENYL SULFONE
CAS Number:4238-09-9
Molecular formula:C9H12O2S
Molecular Weight:184.26

3019-20-3
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$18.00/50g

4238-09-9
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$496.49/5MG

Yield:4238-09-9 100%

Reaction Conditions:

with oxygen in lithium hydroxide monohydrate at 20; under 15001.5 Torr; for 0.333333 h;Sonication;Green chemistry;

Steps:

2.5. General procedure for oxidation of sulfides

General procedure: Reactions were performed at r.t. and in the open air inside a25 mL flask equipped with a magnetic stirrer bar or under US irradiation(100 w). A mixture of sulfides (1 mmol) and DFNSILMo368(0.79 mg) was stirred under the open air at r.t. for therequired time. The reaction procedure was observed by TLC andproduct efficiencies were specified through GC analysis. The productswere purified by chromatography over silica gel (Eluent: ethylacetate/n-hexane 40:60 for sulfoxides isolation and 15:85 for sulfonesisolation). The products were specified using their IR andNMR spectra or compared with the retention time of authenticGC samples.

References:

Xiao, BoAn;Sadeghzadeh, Seyed Mohsen [Journal of Molecular Liquids,2022,vol. 363,art. no. 119921]

5535-48-8 Synthesis