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229308-51-4

Isoxazolo[4,3-c]pyridin-4(5H)-one, 3-methyl- (9CI) synthesis

4synthesis methods
Isoxazolo[4,3-c]pyridin-4(5H)-one, 6,7-dihydro-3-methyl- (9CI)

229308-47-8
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Isoxazolo[4,3-c]pyridin-4(5H)-one, 3-methyl- (9CI)

229308-51-4
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Yield:229308-51-4 82%

Reaction Conditions:

Stage #1: 3-methyl-4,5,6,7-tetrahydroisoxazolo[4,3-c]pyridin-4-onewith tert-butylhypochlorite in methanol at 0;
Stage #2: in methanol; for 0.166667 h;Photolysis;

References:

Jones, Raymond C.F.;Choudhury, Abdul K.;Iley, James N.;Loizou, Georgia;Lumley, Christopher;McKee, Vickie [Synlett,2010,# 4,art. no. D33809ST,p. 654 - 658] Location in patent:scheme or table