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ChemicalBook CAS DataBase List L-Valine Orlistat

L-Valine Orlistat synthesis

1synthesis methods
Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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2258-42-6 Synthesis
Formyl acetate

2258-42-6
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Yield: 57%

Reaction Conditions:

with triethylamine in dichloromethane at 20; for 0.25 h;

References:

Ortar, Giorgio;Bisogno, Tiziana;Ligresti, Alessia;Morera, Enrico;Nalli, Marianna;Di Marzo, Vincenzo [Journal of Medicinal Chemistry,2008,vol. 51,# 21,p. 6970 - 6979] Location in patent:experimental part