m90102 synthesis
- Product Name:m90102
- CAS Number:1011-43-4
- Molecular formula:C10H13NO2
- Molecular Weight:179.22
63909-29-5
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1011-43-4
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Yield:-
Steps:
Multi-step reaction with 6 steps
1: sodium tetrahydroborate / 1,4-dioxane; N,N-dimethyl-formamide / 6 h / 0 - 20 °C
2: nickel; hydrazine hydrate / water; methanol / 1 h / 0 - 40 °C
3: triethylamine / dichloromethane / 4 h / 0 - 20 °C
4: toluene-4-sulfonic acid / toluene / 4 h / 120 °C
5: sodium hydroxide / water; ethanol / 16 h / 120 °C
6: palladium 10% on activated carbon; hydrogen / methanol / 20 °C
References:
Leese, Mathew P.;Jourdan, Fabrice L.;Major, Meriel R.;Dohle, Wolfgang;Hamel, Ernest;Ferrandis, Eric;Fiore, Ann;Kasprzyk, Philip G.;Potter, Barry V. L. [ChemMedChem,2014,vol. 9,# 1,p. 85 - 108]
98809-69-9
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1011-43-4
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36455-21-7
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55161-43-8
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1011-43-4
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124066-12-2
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1011-43-4
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