Methyl 3-broMocyclobutane-1-carboxylate synthesis
- Product Name:Methyl 3-broMocyclobutane-1-carboxylate
- CAS Number:4935-00-6
- Molecular formula:C6H9BrO2
- Molecular Weight:193.04
23761-23-1
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4935-00-6
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 0 - 20 °C / Inert atmosphere
2: sodium tetrahydroborate; methanol / 0.5 h / 0 °C / Inert atmosphere
3: carbon tetrabromide; lithium bromide; triphenylphosphine / tetrahydrofuran / 48 h / 0 - 20 °C / Inert atmosphere
References:
Shindo, Naoya;Ojida, Akio;Tokunaga, Keisuke;Sato, Mami;Kuwata, Keiko;Miura, Chizuru;Fuchida, Hirokazu;Matsunaga, Naoya;Koyanagi, Satoru;Ohdo, Shigehiro [Journal of the American Chemical Society,2020,vol. 142,# 43,p. 18522 - 18531]
4934-99-0
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4935-00-6
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4934-98-9
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$37.00/250mg
4935-00-6
64 suppliers
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1000210-73-0
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4935-00-6
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$38.00/250mg
4958-02-5
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$29.00/1g
4935-00-6
64 suppliers
$38.00/250mg