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128460-74-2

methyl 3'-methylbiphenyl-3-carboxylate synthesis

4synthesis methods
-

Yield:158619-46-6 97%

Steps:

G Experimental

G. 3-Methyl-3'-tert-butoxycarbonylbiphenyl (19). The coupling of 3-methylphenylboronic acid with 3-bromobenzoic acid methyl ester gave a 3-methyl-3'-methoxycarbonylbiphenyl (79% yield), which was then hydrolyzed to yield a 3-methyl-3'-carboxybiphenyl (97% yield).

References:

US5965539,1999,A