Methyl 4-(4-chlorophenyl)-3-oxobutanoate synthesis
- Product Name:Methyl 4-(4-chlorophenyl)-3-oxobutanoate
- CAS Number:1048916-89-7
- Molecular formula:C11H11ClO3
- Molecular Weight:226.66
79-20-9
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Yield:1048916-89-7 34%
Reaction Conditions:
Stage #1: acetic acid methyl esterwith lithium diisopropyl amide in tetrahydrofuran;Inert atmosphere;Cooling;
Stage #2: 4-chlorophenacetyl chloride in tetrahydrofuran at -78 - 20;Inert atmosphere;
References:
Adeel, Muhammad;Rashid, Muhammad A.;Rasool, Nasir;Ahmad, Rasheed;Villinger, Alexander;Reinke, Helmut;Fischer, Christine;Langer, Peter [Synthesis,2009,# 2,p. 243 - 250] Location in patent:experimental part
25026-34-0
150 suppliers
$15.00/1g
1048916-89-7
7 suppliers
inquiry