
METHYL-4 7 8 9-TETRA-O-ACETYL-2-THIO -N- synthesis
- Product Name:METHYL-4 7 8 9-TETRA-O-ACETYL-2-THIO -N-
- CAS Number:116450-06-7
- Molecular formula:C21H31NO12S
- Molecular Weight:521.54
Yield:116450-06-7 91%
Reaction Conditions:
Stage #1: 2-Thiosialic acid methyl ester peracetatewith methanol;sodium at -40; for 0.666667 h;
Stage #2: methyl iodide in N,N-dimethyl-formamide at 20;
References:
Harrison, Jennifer A.;Kartha;Turnbull;Scheuerl, Shona L.;Naismith, James H.;Schenkman, Sergio;Field, Robert A. [Bioorganic and Medicinal Chemistry Letters,2001,vol. 11,# 2,p. 141 - 144]

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