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ChemicalBook CAS DataBase List METHYL 4-METHYL-2-OXOCYCLOPENTANECARBOXYLATE
4463-75-6

METHYL 4-METHYL-2-OXOCYCLOPENTANECARBOXYLATE synthesis

2synthesis methods
2758-18-1 Synthesis
3-methylcyclopent-2-en-1-one

2758-18-1
242 suppliers
$9.00/1g

-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: lithium diisopropyl amide / tetrahydrofuran / 1.33 h / -78 °C / Inert atmosphere
1.2: 3.33 h / -78 - 20 °C
2.1: hydrogen; palladium 10% on activated carbon / methanol / 1 h / 20 °C / Inert atmosphere

References:

WO2018/119208,2018,A1