METHYL (E)-6-METHYLHEPT-4-ENOATE synthesis

1synthesis methods

Product Name:METHYL (E)-6-METHYLHEPT-4-ENOATE
CAS Number:112375-56-1
Molecular formula:C9H16O2
Molecular Weight:156.2221

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Yield:-

Steps:

Multi-step reaction with 3 steps
1: pyridinium chlorochromate (PCC), sodium acetate / CH₂Cl₂ / 1.5 h / Ambient temperature
3: Na(Hg), MeOH / tetrahydrofuran / 8 h / -20 °C

References:

Gannett, Peter M.;Nagel, Donald L.;Reilly, Pam J.;Lawson, Terence;Sharpe, Jody;Toth, Bela [Journal of Organic Chemistry,1988,vol. 53,# 5,p. 1064 - 1071]

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