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82975-96-0

Mono(2-ethyl-6-hydroxyhexyl) Phthalate synthesis

2synthesis methods
-

Yield:82975-96-0 89%

Reaction Conditions:

Stage #1: mono(2-ethyl-5-hexenyl) 1,2-benzenedicarboxylatewith diborane in tetrahydrofuran at 0 - 20;
Stage #2: with sodium hydroxide;dihydrogen peroxide in tetrahydrofuran at 50; for 1 h;

References:

Nuti, Francesca;Hildenbrand, Sibylle;Chelli, Mario;Wodarz, Roman;Papini, Anna Maria [Bioorganic and Medicinal Chemistry,2005,vol. 13,# 10,p. 3461 - 3465]