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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List N-(2-chloro-5-luoropyridin-4-yl)nitraMide
405230-86-6

N-(2-chloro-5-luoropyridin-4-yl)nitraMide synthesis

4synthesis methods
31301-51-6 Synthesis
2-Chloro-5-fluoropyridine

31301-51-6
320 suppliers
$10.00/1g

N-(2-chloro-5-luoropyridin-4-yl)nitraMide

405230-86-6
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: 3.6 g / TFA; aq. H2O2 / 20 h / 70 - 75 °C
2: 59 percent / conc. H2SO4; KNO3 / 2 h / 120 °C
3: 91 percent / H2 / Raney Ni / ethanol / 3 h / 2068.59 Torr
4: 83 percent / conc. H2SO4; KNO3 / 0 - 20 °C

References:

Liu;Luo;Mozdziesz;Lin;Dutschman;Gullen;Cheng;Sartorelli [Nucleosides, nucleotides and nucleic acids,2001,vol. 20,# 12,p. 1975 - 2000]

89510-90-7 Synthesis
4-amino-2-chloro-5-fluoropyridine

89510-90-7
84 suppliers
$27.00/100mg

N-(2-chloro-5-luoropyridin-4-yl)nitraMide

405230-86-6
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References
405230-79-7 Synthesis
Pyridine, 2-chloro-5-fluoro-, 1-oxide (9CI)

405230-79-7
48 suppliers
$40.00/250mg

N-(2-chloro-5-luoropyridin-4-yl)nitraMide

405230-86-6
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References
2-chloro-5-fluoro-4-nitropyridine 1-oxide

405230-80-0
30 suppliers
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N-(2-chloro-5-luoropyridin-4-yl)nitraMide

405230-86-6
5 suppliers
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References