N-(4-acetyl-3,5-dimethylphenyl)acetamide synthesis
- Product Name:N-(4-acetyl-3,5-dimethylphenyl)acetamide
- CAS Number:100923-73-7
- Molecular formula:C12H15NO2
- Molecular Weight:205.25
Yield:100923-73-7 98%
Reaction Conditions:
Stage #1: N-acetyl-3,5-dimethylanilinewith aluminum (III) chloride in dichloromethane at 0;Inert atmosphere;
Stage #2: acetyl chloride in dichloromethane at 0; for 3 h;Inert atmosphere;
References:
álvarez, Eleuterio;álvarez, Mariá;Fructos, Manuel R.;Lledós, Agustí;Molina, Francisco;Pérez, Pedro J.;Sodupe, Mariona;Urbano, Juan [Dalton Transactions,2020,vol. 49,# 41,p. 14647 - 14655] Location in patent:supporting information
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