N-Benzylidene-1-napthylamine synthesis
- Product Name:N-Benzylidene-1-napthylamine
- CAS Number:890-51-7
- Molecular formula:C17H13N
- Molecular Weight:231.29
Yield:890-51-7 100%
Reaction Conditions:
with aluminum(III) oxide for 5 h;Milling;
Steps:
Aldimines 2a-g, 4; General Procedure
General procedure: The required amine (10 mmol) was stirred with slow-basic chromatographic Al2O3 (3 g). Aldehyde (10 mmol for 2a-g or 20 mmol for 4) was stirred with slow-basic chromatographic Al2O3 (3 g). The aldehyde dispersed on alumina was added by portions to the amine dispersed on alumina upon grinding and then the mixture was allowed to stay for 5 h. The aldimine formed was extracted with CH2Cl2 (2 × 25 mL) and the combined extracts were evaporated under reduced pressure to give the desired product in almost quantitative yield.
References:
Arbuzova, Svetlana N.;Gusarova, Nina K.;Kazantseva, Tatyana I.;Kolyvanov, Nikita A.;Trofimov, Boris A.;Verkhoturova, Svetlana I.;Zinchenko, Sergey V. [Synthesis,2020,vol. 52,# 10,p. 1531 - 1540]
6361-33-7
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