N-BOC-3-(3-METHYL-4-NITROBENZYL)-L- synthesis

1synthesis methods

Product Name:N-BOC-3-(3-METHYL-4-NITROBENZYL)-L-
CAS Number:114787-83-6
Molecular formula:C20H26N4O6
Molecular Weight:418.44

80866-75-7
92 suppliers
$23.00/1g

114787-83-6
12 suppliers
$179.00/1g

Yield:-

Steps:

Multi-step reaction with 2 steps
1: (iPr)2NEt / CH₂Cl₂ / 0.5 h / -75 °C
2: 1.) CH₂Cl₂, from -75 deg C to RT, 8 h, 2.) CH₂Cl₂, pH 7, 1.5 h

References:

Blankley, C. John;Hodges, John C.;Klutchko, Sylvester R.;Himmelsbach, Richard J.;Chucholowski, Alexander;et al. [Journal of Medicinal Chemistry,1991,vol. 34,# 11,p. 3248 - 3260]