N-Boc-D-phenylalanine N'-Methoxy-N'-MethylaMide synthesis
- Product Name:N-Boc-D-phenylalanine N'-Methoxy-N'-MethylaMide
- CAS Number:115186-33-9
- Molecular formula:C16H24N2O4
- Molecular Weight:308.37
18942-49-9
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Yield:115186-33-9 98%
Reaction Conditions:
Stage #1: Boc-D-Phe-OHwith triethylamine in dichloromethane;Inert atmosphere;
Stage #2: with (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphateInert atmosphere;
Stage #3: N,O-dimethylhydroxylamine*hydrochloridewith triethylamineInert atmosphere;
References:
Cai, Xiaoqing;Zaleski, Paul A.;Cagir, Ali;Hecht, Sidney M. [Bioorganic and Medicinal Chemistry,2011,vol. 19,# 12,p. 3831 - 3844] Location in patent:scheme or table
13734-34-4
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115186-33-9
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