N-butyl-3-nitrobenzamide synthesis
- Product Name:N-butyl-3-nitrobenzamide
- CAS Number:70001-47-7
- Molecular formula:C11H14N2O3
- Molecular Weight:222.24
Yield: 78%
Reaction Conditions:
with cobalt oxide nanoparticles Co/SBA-15 at 70; for 4 h;
Steps:
2.3. Amidation reactions
General procedure: The amidation reaction was first conducted between benzaldehyde, piperidine, CoNP (0.5 mol.%) as catalyst, and hydrogen peroxide as oxidant. The reaction was conducted at 70 °C for 1-5 h depending on the substrates. Subsequently, the catalyst was tested with various substrates and nitrogen precursors.
References:
Rajabi, Fatemeh;Raessi, Mojdeh;Arancon, Rick A.D.;Saidi, Mohammad Reza;Luque, Rafael [Catalysis Communications,2015,vol. 59,p. 122 - 126]
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