N-methoxy-N-methyl-2-nitrobenzamide synthesis
- Product Name:N-methoxy-N-methyl-2-nitrobenzamide
- CAS Number:339221-51-1
- Molecular formula:C9H10N2O4
- Molecular Weight:210.19
552-16-9
374 suppliers
$10.00/10g
6638-79-5
589 suppliers
$6.00/25g
339221-51-1
23 suppliers
inquiry
Yield:339221-51-1 95%
Reaction Conditions:
Stage #1: ortho-nitrobenzoic acidwith 4-methyl-morpholine;4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride in tetrahydrofuran at 20; for 1.5 h;
Stage #2: N,O-dimethylhydroxylamine*hydrochloride in tetrahydrofuran at 20; for 8 h;Further stages.;
References:
De Luca;Giacomelli;Taddei [Journal of Organic Chemistry,2001,vol. 66,# 7,p. 2534 - 2537]
6638-79-5
589 suppliers
$6.00/25g
199620-15-0
0 suppliers
inquiry
342589-38-2
0 suppliers
inquiry
339221-51-1
23 suppliers
inquiry