N-PYRIDIN-3-YLPROPANE-1,3-DIAMINE synthesis

1synthesis methods

Product Name:N-PYRIDIN-3-YLPROPANE-1,3-DIAMINE
CAS Number:938459-11-1
Molecular formula:C8H13N3
Molecular Weight:151.21

462-08-8 Synthesis

462-08-8
473 suppliers
$14.00/25g

156-87-6
479 suppliers
$5.00/10g

938459-11-1
9 suppliers
$70.00/1g

Yield:938459-11-1 75%

Reaction Conditions:

with bis(1,5-cyclooctadiene)diiridium(I) dichloride;Py₂NPiPr₂;sodium t-butanolate in tetrahydrofuran;diethylene glycol dimethyl ether at 110; for 24 h;Inert atmosphere;chemoselective reaction;

References:

Blank, Benoit;Michlik, Stefan;Kempe, Rhett [Advanced Synthesis and Catalysis,2009,vol. 351,# 17,p. 2903 - 2911] Location in patent:experimental part

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