ChemicalBook CAS DataBase List N1-[2-AMINO-4-(TRIFLUOROMETHYL)PHENYL]ACETAMIDE

N1-[2-AMINO-4-(TRIFLUOROMETHYL)PHENYL]ACETAMIDE synthesis

2synthesis methods

Product Name:N1-[2-AMINO-4-(TRIFLUOROMETHYL)PHENYL]ACETAMIDE
CAS Number:97051-69-9
Molecular formula:C9H9F3N2O
Molecular Weight:218.18

Acetamide, N-[2-nitro-4-(trifluoromethyl)phenyl]-

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N1-[2-AMINO-4-(TRIFLUOROMETHYL)PHENYL]ACETAMIDE

97051-69-9
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Yield:-

Reaction Conditions:

with palladium on activated charcoal;hydrogen in methanol at 20; under 2585.81 Torr; for 0.333333 h;

Steps:

33.2

Step 2. The crude product from the previous step was dissolved in MeOH (20 mL) and Pd/C (catalytic) was added. The reaction mixture was shaken at room temperature under hydrogen (50 psi) for 20 minutes, then filtered through Celite. The product was concentrated and made into the azeotrope using toluene to provide crude N-(2-amino-4- (trifluoromethyl)phenyl) acetamide.

References:

WO2015/76800,2015,A1 Location in patent:Page/Page column 208

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97051-69-9
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$28.60/50mg

References