N1-BENZYL-N1-METHYLETHANE-1,2-DIAMINE synthesis
- Product Name:N1-BENZYL-N1-METHYLETHANE-1,2-DIAMINE
- CAS Number:14165-18-5
- Molecular formula:C10H16N2
- Molecular Weight:164.25
17542-47-1
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Yield: 84%
Reaction Conditions:
with ammonium hydroxide at 40;Sealed tube;
Steps:
1; 4 Compound 3
The compound 2 (20 g, 108.9 mmol) and 215 mL of ammonia water were added into a 500 mL sealed tube, the mixed solution was stirred at 40°C overnight, TLC was performed to ensure that no raw materials remained, and the product was purified by column chromatography to obtain 15 g of colorless liquid, i.e., compound 3, yield 84%.
References:
Nanjing Chuangte Pharmaceutical Technology Co., Ltd;ZHU, Yongqiang;LIU, Zhaogang;FENG, Chao;HU, Shihe;CHEN, Hao;BAI, Enhe;WANG, Jia;SHI, Jingmiao EP3498708, 2019, A1 Location in patent:Paragraph 0025; 0026; 0031; 0032; 0079; 0080; 0085; 0086
14321-25-6
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574-98-1
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103-67-3
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103-67-3
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14165-18-5
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101-98-4
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14165-18-5
71 suppliers
$45.00/50mg