N2-Cyclopropyl-4-Methyl-2,3-pyridinediaMine synthesis
- Product Name:N2-Cyclopropyl-4-Methyl-2,3-pyridinediaMine
- CAS Number:284686-18-6
- Molecular formula:C9H13N3
- Molecular Weight:163.22
284686-17-5
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284686-18-6
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Yield:284686-18-6 83%
Reaction Conditions:
Stage #1: 2-(cyclopropylamino)-4-methyl-3-nitropyridinewith hydrogenchloride;tin(II) chloride dihdyrate;acetic acid in water at 20;
Stage #2: with sodium hydroxide in water; pH=12;Cooling with ice;
References:
Khunnawutmanotham, Nisachon;Chimnoi, Nitirat;Techasakul, Supanna;Thitithanyanont, Arunee;Saparpakorn, Patchreenart;Hannongbua, Supa;Choowongkomon, Kiattawee;Pungpo, Pornpan [Beilstein Journal of Organic Chemistry,2009,vol. 5,art. no. A36] Location in patent:supporting information; experimental part
23056-39-5
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284686-18-6
8 suppliers
$85.00/10mg