N2-Isobutyl-2,3-pyridinediamine synthesis
- Product Name:N2-Isobutyl-2,3-pyridinediamine
- CAS Number:1021284-13-8
- Molecular formula:C9H15N3
- Molecular Weight:165.24
942356-83-4
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1021284-13-8
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Yield:1021284-13-8 85%
Reaction Conditions:
with palladium on activated carbon;ammsnium formate at 60;Microwave irradiation;
Steps:
2.1.3. general method for preparation of compounds 6-7
General procedure: Compounds 6-7 were prepared using microwave irradiation in pyrex microwave cuvettes using 5 w% of Pd/C and ammonium formate as source of hydrogen. Reaction mixture was irradiated for few minutes at 60 °C with power 300 W until TLC indicated end of reaction. After cooling, the reaction mixture was filtered over acelite bed and filtrate was evaporated at a reduced pressure. Compounds were used in the next step without further purification.
References:
Bo?ek, Ida;Star?evi?, Kristina;Novak Jovanovi?, Ivana;Vianello, Robert;Hranjec, Marijana [Journal of Molecular Liquids,2021,vol. 342,art. no. 117527]
5470-18-8
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1021284-13-8
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