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ChemicalBook CAS DataBase List N3-PEG6-CH2COOH
880129-82-8

N3-PEG6-CH2COOH synthesis

6synthesis methods
Azido-PEG6-CH2CO2t-butyl ester

297162-49-3
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N3-PEG6-CH2COOH

880129-82-8
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Yield:880129-82-8 79%

Reaction Conditions:

with trifluoroacetic acid in dichloromethane at 0 - 20; for 6 h;

References:

Sato, Ryota;Kozuka, Jun;Ueda, Masahiro;Mishima, Reiko;Kumagai, Yutaro;Yoshimura, Akimasa;Minoshima, Masafumi;Mizukami, Shin;Kikuchi, Kazuya [Journal of the American Chemical Society,2017,vol. 139,# 48,p. 17397 - 17404] Location in patent:supporting information