Nepetoidin B synthesis
1synthesis methods
- Product Name:Nepetoidin B
- CAS Number:55486-06-1
- Molecular formula:C17H14O6
- Molecular Weight:314.29
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: carbon tetrabromide; triisopropyl phosphate / 0.58 h / 0 °C
1.2: 0.83 h / 0 - 25 °C
2.1: bis(2-methylpropenyl) / toluene / 12 h / 45 °C / Inert atmosphere
3.1: quinoline; trimethylsilyl iodide / 4 h / 0 - 175 °C / Inert atmosphere
References:
Xiong, Hangxing;Yang, Sen;Yao, Ming;Zhang, Jingjing [ARKIVOC,2020,vol. 2020,# 6]