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NICOTINOYL AZIDE synthesis

11synthesis methods
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Yield:4013-72-3 89%

Reaction Conditions:

with Caswell No. 744A;trichloroacetonitrile;triphenylphosphine in propan-2-one at 20; for 0.5 h;Inert atmosphere;

References:

Kim, Joong-Gon;Jang, Doo Ok [Synlett,2008,# 13,p. 2072 - 2074] Location in patent:experimental part