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ChemicalBook CAS DataBase List Nonylphosphonic acid
4730-79-4

Nonylphosphonic acid synthesis

2synthesis methods
-

Yield:4730-79-4 71%

Reaction Conditions:

Stage #1: 1-Bromononanewith potassium hydroxide semihydrate;phosphorus;cetyltrimethylammonim bromide in water;toluene at 85 - 90; for 6 h;Inert atmosphere;
Stage #2: with nitric acid in water at 100 - 110; pH=4; for 2 h;Inert atmosphere;

References:

Kuimov, Vladimir A.;Malysheva, Svetlana F.;Belogorlova, Natalia A.;Albanov, Alexander I.;Gusarova, Nina K.;Trofimov, Boris A. [European Journal of Organic Chemistry,2021,vol. 2021,# 10,p. 1596 - 1602] Location in patent:supporting information