Norvaline, 3-ethyl-N-[(phenylmethoxy)carbonyl]- synthesis
- Product Name:Norvaline, 3-ethyl-N-[(phenylmethoxy)carbonyl]-
- CAS Number:785735-06-0
- Molecular formula:C15H21NO4
- Molecular Weight:279.33
97-96-1
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: sodium hydrogensulfite / methanol; water / 12 h / 60 °C
2: hydrogen bromide / 2 h / 150 °C
3: sodium hydroxide / 17 h / 20 °C
References:
Saito, Tetsuji;Obitsu, Tetsuo;Kohno, Hiroshi;Sugimoto, Isamu;Matsushita, Takeshi;Nishiyama, Taihei;Hirota, Tomoko;Takeda, Hiroyuki;Matsumura, Naoya;Ueno, Sonoko;Kishi, Akihiro;Kagamiishi, Yoshifumi;Nakai, Hisao;Takaoka, Yoshikazu [Bioorganic and Medicinal Chemistry,2012,vol. 20,# 2,p. 1122 - 1138]
110072-96-3
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