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ChemicalBook CAS DataBase List NSC 38280

NSC 38280 synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 4 h / Cooling with ice
2: sodium acetate / toluene; acetic acid / 20 °C / Inert atmosphere

References:

Haynes, Keith M.;Abdali, Narges;Jhawar, Varsha;Zgurskaya, Helen I.;Parks, Jerry M.;Green, Adam T.;Baudry, Jerome;Rybenkov, Valentin V.;Smith, Jeremy C.;Walker, John K. [Journal of Medicinal Chemistry,2017,vol. 60,# 14,p. 6205 - 6219]

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