o-(triisopropylsilyl)hydroxylaMine synthesis

1synthesis methods

Product Name:o-(triisopropylsilyl)hydroxylaMine
CAS Number:1170696-39-5
Molecular formula:C9H23NOSi
Molecular Weight:189.37

13154-24-0 Synthesis

13154-24-0
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1170696-39-5
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Yield:1170696-39-5 84.5%

Reaction Conditions:

with hydroxylamine hydrochloride;triethylamine in dichloromethane at 20; for 75 h;Inert atmosphere;

References:

Dong, Xichang;Kita, Yuji;Oestreich, Martin [Angewandte Chemie - International Edition,2018,vol. 57,# 33,p. 10728 - 10731][Angew. Chem.,2018,vol. 130,# 33,p. 10888 - 10891,4] Location in patent:supporting information

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