oxanthranol synthesis
- Product Name:oxanthranol
- CAS Number:4981-66-2
- Molecular formula:C14H10O2
- Molecular Weight:210.23
84-65-1
4981-66-2
The general procedure for the synthesis of 9,10-anthracenediol from anthraquinone was as follows: a mixture of anthraquinone (104 mg, 0.5 mmol) and sodium sulfide nonahydrate (480 mg, 2.0 mmol) in ethanol (30 mL) was reacted for 2 h at 78 °C with stirring under argon protection. Upon completion of the reaction, the mixture was cooled to 10 °C and the unreacted anthraquinone was removed by rapid filtration to afford the product 9,10-anthracenediol with a mass of 93 mg (90% yield). The anthraquinone present in the filtrate was oxidized and precipitated in air to give a final 10 mg (10% yield).
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: carbon tetrachloride; iodine; chlorine
2: acetone; water
3: water / Darst.
References:
Matthews [Journal of the Chemical Society,1926,p. 243]
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4981-66-2
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4981-66-2
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$5.00/100mg
4981-66-2
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$87.00/250mg
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