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ChemicalBook CAS DataBase List Peachflure
63408-44-6

Peachflure synthesis

12synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 1.) aluminum chloride; 2.) sodium methoxide / 1.) methylene dichloride, room temp., 3 h; 2.) methanol, reflux, 8 h
2: 93 percent / pentane / 0.5 h
3: 1.) butyllithium / 1.) THF, hexane, 20-25 deg C, 30 min; 2.) 20-25 deg C, 2 h

References:

Kulinkovich, O. G.;Tishchenko, I. G.;Sorokin, V. L. [Journal of Organic Chemistry USSR (English Translation),1986,vol. 22,# 9,p. 1638 - 1640][Zhurnal Organicheskoi Khimii,1986,vol. 22,# 9,p. 1825 - 1827]

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