PENTA-L-PHENYLALANINE ACETATE SALT synthesis
- Product Name:PENTA-L-PHENYLALANINE ACETATE SALT
- CAS Number:65757-10-0
- Molecular formula:C45H47N5O6
- Molecular Weight:753.88
13734-34-4
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65757-10-0
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$595.71/10MG
Yield:-
Steps:
Multi-step reaction with 9 steps
1.1: benzotriazol-1-ol / N,N-dimethyl-formamide / 0.25 h / 0 °C
1.2: 0.08 h / 0 °C
1.3: 24 h / 0 - 20 °C
2.1: trifluoroacetic acid / dichloromethane / 2.25 h / 0 - 20 °C / Inert atmosphere
3.1: benzotriazol-1-ol / N,N-dimethyl-formamide / 0.25 h / 0 °C
3.2: 0.08 h / 0 °C
3.3: 24 h / 0 - 20 °C
4.1: palladium 10% on activated carbon; hydrogen / ethanol / 2 h
5.1: benzotriazol-1-ol / N,N-dimethyl-formamide / 0.25 h / 0 °C
5.2: 0.08 h / 0 °C
5.3: 24 h / 0 - 20 °C
6.1: palladium 10% on activated carbon; hydrogen / ethanol / 2 h
7.1: benzotriazol-1-ol / N,N-dimethyl-formamide / 0.25 h / 0 °C
7.2: 0.08 h / 0 °C
7.3: 24 h / 0 - 20 °C
8.1: palladium 10% on activated carbon; hydrogen / ethanol / 2 h
9.1: lithium hydroxide monohydrate / methanol; water / 2 h / 20 °C
References:
Cindro, Nikola;Horvat, Gordan;Rinkovec, Tamara;Riva, Davide;Speranza, Giovanna;Tomi?i?, Vladislav;Vidovi?, Nikolina [Organic Letters,2020]
2577-90-4
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65757-10-0
31 suppliers
$595.71/10MG
13122-89-9
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65757-10-0
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17528-17-5
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65757-10-0
31 suppliers
$595.71/10MG