(Perfluorohexyl)ethylene synthesis
- Product Name:(Perfluorohexyl)ethylene
- CAS Number:25291-17-2
- Molecular formula:C8H3F13
- Molecular Weight:346.09
2043-57-4
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25291-17-2
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Yield:25291-17-2 97.6%
Reaction Conditions:
with tetrabutylammomium bromide;sodium hydrogencarbonate in water at 20; for 24 h;Reagent/catalyst;Temperature;
Steps:
3 Example 1
To the reaction flask was added 3.01 g (0.036 mol) of sodium bicarbonate, 7.5 g (0.42 mol) of deionized water, 1.54 g (0.00478 mol) of tetrabutylammonium bromide and 10.01 g (0.021 mol) of perfluorohexylethyl iodide at 20 ° C The reaction was stirred for 24 hours, standing stratification, common deionized water 15ml wash the lower organic phase three times. 7.13 g of perfluorohexylethylene was obtained in a yield of 97.6%.
References:
CN105837397,2016,A Location in patent:Paragraph 0028-0030
1374104-95-6
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6900-35-2
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2144-53-8
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6900-35-2
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647-42-7
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25291-17-2
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108-59-8
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