perilla ketone synthesis
- Product Name:perilla ketone
- CAS Number:553-84-4
- Molecular formula:C10H14O2
- Molecular Weight:166.22
498-60-2
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: 71 percent / H2SO4 / ethanol; tetrahydrofuran / 3 h / Ambient temperature
2: n-BuLi / tetrahydrofuran; cyclohexane / 1.) -78 deg C, 2.) -78 deg C, 2 min
3: aq. HCl / tetrahydrofuran / Ambient temperature
References:
Katritzky, Alan R.;Lang, Hengyuan;Wang, Zuoquan;Zhang, Zhongxing;Song, Huimin [Journal of Organic Chemistry,1995,vol. 60,# 23,p. 7619 - 7624]
107-82-4
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