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ChemicalBook CAS DataBase List Phen-2,3,4,5-d4-ol, 6-amino-
121887-11-4

Phen-2,3,4,5-d4-ol, 6-amino- synthesis

2synthesis methods
-

Yield:121887-11-4 71%

Reaction Conditions:

Stage #1: 2-amino-phenolwith platinum on carbon;hydrogen;water-d2 at 180; for 24 h;
Stage #2: with water in diethyl ether;

References:

Ito, Nobuhiro;Esaki, Hiroyoshi;Maesawa, Tsuneaki;Imamiya, Eikoh;Maegawa, Tomohiro;Sajiki, Hironao [Bulletin of the Chemical Society of Japan,2008,vol. 81,# 2,p. 278 - 286] Location in patent:experimental part