ChemicalBook CAS DataBase List POLYGODIAL

POLYGODIAL synthesis

4synthesis methods

Product Name:POLYGODIAL
CAS Number:33118-34-2
Molecular formula:C15H22O2
Molecular Weight:234.33

1,2-Naphthalenedicarboxylic acid, 3,5,6,7,8,8a-hexahydro-5,5,8a-trimethyl-, 1,2-dimethyl ester

71557-96-5
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 80 percent / H₂, HCl / 10percent Pd-C / methanol / 760 Torr
2: 90 percent / LiAlH₄
3: 95 percent / (COCl)2, DMSO / 1 h / -50 °C

References:

Howell, S. Christopher;Ley, Steven V.;Mahon, Michael;Worthington, Paul A. [Journal of the Chemical Society. Chemical communications,1981,# 11,p. 507 - 508]

5293-90-3 Synthesis

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References

432-25-7
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References

2-Naphthalenecarboxaldehyde, 3,4,4a,5,6,7,8,8a-octahydro-5,5,8a-trimethyl-3-oxo-, (4aR,8aS)-rel-

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References

POLYGODIAL Related Search:

2,4-DIMETHYL-3-CYCLOHEXENECARBOXALDEHYDE

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