PROPANENITRILE, 3-[(2-AMINOETHYL)AMINO]- synthesis
- Product Name:PROPANENITRILE, 3-[(2-AMINOETHYL)AMINO]-
- CAS Number:22584-31-2
- Molecular formula:C5H11N3
- Molecular Weight:113.16
Yield:22584-31-2 98.5 %Chromat.
Reaction Conditions:
with porous hyper-cross-linked polymer containing 2.87 mmol/g of ionic liquid embedded in framework synthesized from 4-vinylpyridine and p-xylylene dichloride in neat (no solvent) at 25; for 0.116667 h;Michael Addition;
Steps:
The Procedure for aza-Michael Addition
General procedure: Requisite amounts of amines (20 mmol), alkenes (24 mmol) and catalyst (20 mg) were mixed and reacted for definite time intervals at ambient temperature. The GC analysis was conducted to monitor the reaction process. On completion, the catalyst was recycled by filtration. The recycled catalyst was washed with ethanol and dried at 80°C overnight. Activity of the recycled system was carefully investigated.
References:
Li, Junqiao;Lu, Wei;Li, Weifeng;Liang, Xuezheng [Kinetics and Catalysis,2016,vol. 57,# 6,p. 840 - 846]
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![Propanenitrile, 3,3'-[[2-[(2-cyanoethyl)amino]ethyl]imino]bis-](/CAS/20210305/GIF/56576-72-8.gif)
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22584-31-2
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107-15-3
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22584-31-2
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107-15-3
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$11.19/25ML
107-13-1
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$19.00/25ML
3217-00-3
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22584-31-2
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