Pyrazinecarbonyl chloride, 6-chloro- (9CI) synthesis
- Product Name:Pyrazinecarbonyl chloride, 6-chloro- (9CI)
- CAS Number:148673-71-6
- Molecular formula:C5H2Cl2N2O
- Molecular Weight:176.99
6164-79-0
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148673-71-6
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: 3-chloro-benzenecarboperoxoic acid / 1,2-dichloro-ethane / 16 h / 60 °C
2: thionyl chloride / 8 h / Reflux
3: ethanol; sodium hydroxide / 2 h / 20 °C
4: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 3 h / 20 °C
References:
Scanio, Marc J. C.;Shi, Lei;Bunnelle, William H.;Anderson, David J.;Helfrich, Rosalind J.;Malysz, John;Thorin-Hagene, Kirsten K.;Van Handel, Ceclia E.;Marsh, Kennan C.;Lee, Chih-Hung;Gopalakrishnan, Murali [Journal of Medicinal Chemistry,2011,vol. 54,# 21,p. 7678 - 7692]
23688-89-3
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23611-75-8
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770-00-3
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148673-71-6
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98-97-5
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