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ChemicalBook CAS DataBase List PYRENE-1-SULFONIC ACID SODIUM SALT

PYRENE-1-SULFONIC ACID SODIUM SALT synthesis

1synthesis methods
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Yield: 71%

Reaction Conditions:

Stage #1:pyrene with chlorosulfonic acid in dichloromethane at 0; for 2 h;Inert atmosphere;
Stage #2: with sodium hydroxide in dichloromethaneInert atmosphere;

References:

Yan, Ni;Xu, Zhiyan;Diehn, Kevin K.;Raghavan, Srinivasa R.;Fang, Yu;Weiss, Richard G. [Journal of the American Chemical Society,2013,vol. 135,# 24,p. 8989 - 8999] Location in patent:supporting information

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