pyruvamide synthesis
- Product Name:pyruvamide
- CAS Number:631-66-3
- Molecular formula:C3H5NO2
- Molecular Weight:87.08
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Yield: 98.3%
Reaction Conditions:
with ammonia in methanol at 0; for 0.5 h;Solvent;
Steps:
1-4; 1 Example 1: Preparation of 2-oxopropionamide
50 g (430.8 mmol, 1 eq) of ethyl pyruvate at 0 ° CAdd slowly to 250ml of 7M ammonia in methanol solution, and stir at 0 ° C for 30min.A white solid precipitated, filtered with suction, and dried at room temperature to obtain 36.8 g of a white solid.The yield was 98.3%.
References:
Shanghai Pharmaceutical Industry Institute;China Pharmaceutical Industry Zongyuan;Zhang Peng;Cai Zhengyan CN110615751, 2019, A Location in patent:Paragraph 0065-0072; 0081-0082
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