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ChemicalBook CAS DataBase List (R)-1-O-TOLYLETHANAMINE-HCl
856562-88-4

(R)-1-O-TOLYLETHANAMINE-HCl synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 5%-palladium/activated carbon; hydrogen / Isopropyl acetate / 24 h / 24 °C / 11251.1 Torr
2: 5%-palladium/activated carbon; hydrogen / Isopropyl acetate / 24 h / 55 °C
3: hydrogenchloride / dichloromethane; water

References:

Nugent, Thomas C.;Negru, Daniela E.;El-Shazly, Mohamed;Hu, Dan;Sadiq, Abdul;Bibi, Ahtaram;Umar, M. Naveed [Advanced Synthesis and Catalysis,2011,vol. 353,# 11-12,p. 2085 - 2092]