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ChemicalBook CAS DataBase List (R)-2-TERT-BUTYL-6-METHYL-1,3-DIOXIN-4-ONE
107289-20-3

(R)-2-TERT-BUTYL-6-METHYL-1,3-DIOXIN-4-ONE synthesis

2synthesis methods
100017-18-3 Synthesis
(2R,6R)-2-TERT-BUTYL-6-METHYL-1,3-DIOXAN-4-ONE

100017-18-3
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Yield:-

Reaction Conditions:

with N-Bromosuccinimide;2,2'-azobis(isobutyronitrile);hydrogen;triethylamine;palladium1) CCl4, reflux, 3h; 2) EtOH, 6h;Yield given. Multistep reaction;

References:

Zimmermann, Juerg;Seebach, Dieter [Helvetica Chimica Acta,1987,vol. 70,p. 1104 - 1114]