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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
63328-06-3

R-(γ)-Phe synthesis

8synthesis methods
3182-95-4 Synthesis
L-Phenylglycinol

3182-95-4
476 suppliers
$5.00/5g

R-(γ)-Phe

63328-06-3
16 suppliers
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-

Yield:-

Steps:

Multi-step reaction with 5 steps
1: 93 percent / 0.5 h / 135 - 140 °C
2: 98 percent / (COCl)2; DMSO; DIPEA / CH2Cl2 / -45 - -30 °C
3: t-BuOK / tetrahydrofuran / 2 h / 20 °C
4: 1.25 g / NiCl2*6H2O; NaBH4 / methanol; tetrahydrofuran / 0.17 h / -30 °C
5: 95 percent / aq. HCl / dioxane / 15 h / Heating

References:

Nasopoulou, Magdalini;Georgiadis, Dimitris;Matziari, Magdalini;Dive, Vincent;Yiotakis, Athanasios [Journal of Organic Chemistry,2007,vol. 72,# 19,p. 7222 - 7228]

26250-86-2 Synthesis
(S)-3-(((Benzyloxy)carbonyl)amino)-4-phenylbutanoic acid

26250-86-2
11 suppliers
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R-(γ)-Phe

63328-06-3
16 suppliers
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References
Benzenebutanoic acid, β-[[(phenylmethoxy)carbonyl]amino]-, methyl ester, (βS)-

97206-05-8
0 suppliers
inquiry

R-(γ)-Phe

63328-06-3
16 suppliers
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References
(S)-3-Z-AMINO-1-DIAZO-3-PHENYL-2-BUTANONE

15196-02-8
8 suppliers
inquiry

R-(γ)-Phe

63328-06-3
16 suppliers
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References
(R)-4-(BOC-AMINO)-5-PHENYLPENTANOIC ACID

195867-20-0
47 suppliers
$70.00/250mg

R-(γ)-Phe

63328-06-3
16 suppliers
inquiry

References