rel-(8aβ*)-4aα*-Methyldecalin-2-one synthesis
- Product Name:rel-(8aβ*)-4aα*-Methyldecalin-2-one
- CAS Number:938-07-8
- Molecular formula:C11H18O
- Molecular Weight:166.26
487-51-4
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Yield:-
Steps:
Multi-step reaction with 7 steps
1: 36 percent / 1) NaOEt / ethanol / 1) 20 deg C, 30 min, 2) reflux, 4.5 h
2: 13 percent / hydrogen / 11percent Pd/C / diethyl ether / 24 h / 1520 Torr
3: 80 percent / p-TsOH / methanol / 2 h / 20 °C
4: 95 percent / LiAlH4 / tetrahydrofuran / 5 h / Heating
5: 1) n-BuLi / 1) THF, TMEDA, -78 deg C, 2) THF, TMEDA, 25 deg C, 2 h
6: 77 percent / Li, EtNH2, t-BuOH / tetrahydrofuran / 1.5 h / 0 °C
7: 55 percent / 90percent aq. HCOOH / tetrahydrofuran
References:
Jones, J. Bryan;Dodds, David R. [Canadian Journal of Chemistry,1987,vol. 65,p. 2397 - 2404]
826-56-2
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2547-28-6
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![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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