ChemicalBook CAS DataBase List reumycin

reumycin synthesis

9synthesis methods

Product Name:reumycin
CAS Number:5016-18-2
Molecular formula:C6H5N5O2
Molecular Weight:179.14

4318-56-3 Synthesis

4318-56-3
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5016-18-2
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Yield:-

Steps:

Multi-step reaction with 6 steps
1: 69 percent / conc. H₂SO₄, fuming HNO₃ / from 15 deg C to r.t., then r.t. 30 min
2: H₂ / 5percent Pt/C / methanol; aq. NH₃ / 517.1 - 2327.2 Torr
3: CH₂Cl₂ / 0.25 h / below 40 deg C
4: ethanol / 2.5 h / Heating
5: satur. ammonium sulfate / H₂O / 48 h
6: 38 percent / dimethylformamide / 4.5 h / Heating

References:

Black [Journal of Heterocyclic Chemistry,1987,vol. 24,# 5,p. 1373 - 1375]

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References

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6945-56-8
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References

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References

84-82-2
67 suppliers
$25.00/1mg

5016-18-2
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References

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