rhodiocyanoside A synthesis
- Product Name:rhodiocyanoside A
- CAS Number:168433-86-1
- Molecular formula:C11H17NO6
- Molecular Weight:259.26
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Yield:-
Steps:
Multi-step reaction with 5 steps
1: 25 percent / β-glucosidase, phosphate buffer, pH 5 / 24 h / 30 °C
2: 98 percent / pyridine, 4-dimethylaminopyridine / 0.25 h / Ambient temperature
3: 1.) O3, 2.) Me2S / 1.) CH2Cl2, -78 deg C, 2 h, 2.) CH2Cl2, RT, 30 min
4: 1.) NaH / 1.) n-hexane, THF, 0 deg C, 15 min, 2.) n-hexane, THF, 0 deg C, 30 min
5: 77 percent / K2CO3 / methanol / 0.5 h / Ambient temperature
References:
Akita, Hiroyuki;Kurashima, Katsumi;Nakamura, Takuya;Kato, Keisuke [Tetrahedron Asymmetry,1999,vol. 10,# 12,p. 2429 - 2439]
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168433-86-1
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