S-(1,1-Dioxothiolan-3-yl) ethanethioate synthesis
1synthesis methods
- Product Name:S-(1,1-Dioxothiolan-3-yl) ethanethioate
- CAS Number:201990-25-2
- Molecular formula:C6H10O3S2
- Molecular Weight:194.27
Yield:201990-25-2 30%
Reaction Conditions:
with 2,2'-azobis(isobutyronitrile) in toluene at 100; for 15 h;Inert atmosphere;
References:
Li, Bryan;Buzon, Richard A.;Hritzko, Benjamin [Synlett,2012,# 1,art. no. S08911ST,p. 131 - 133] Location in patent:experimental part