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110220-54-7

(S)-2,2-Dimethyl-1,3-dioxolane-4-methanol-d2 synthesis

3synthesis methods
52373-72-5 Synthesis
(R)-(+)-2,2-DIMETHYL-1,3-DIOXOLANE-4-CARBOXYLIC ACID METHYL ESTER

52373-72-5
146 suppliers
$12.00/1g

(S)-2,2-Dimethyl-1,3-dioxolane-4-methanol-d2

110220-54-7
2 suppliers
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Yield:110220-54-7 98%

Reaction Conditions:

with sodium borodeuteride in tetrahydrofuran;deuteromethanol at 0 - 20; for 13 h;Inert atmosphere;

References:

Martin, Christopher J.;Lee, Alan T. L.;Adams, Ralph W.;Leigh, David A. [Journal of the American Chemical Society,2017,vol. 139,# 34,p. 11998 - 112002] Location in patent:supporting information